二硫化铼超薄纳米片的制备及其在调Q掺铒光纤激光器中的应用

何俊杉; 曾国华; 刘绍贤; 卢海明; 谢锐贤; 戚晶晶; 陶丽丽; 周博

doi:10.1631/FITEE.2000339

Your Location：

Home >

Browse articles >

二硫化铼超薄纳米片的制备及其在调Q掺铒光纤激光器中的应用

超快低维材料器件及其调控专题 | Updated：2022-05-19

- 二硫化铼超薄纳米片的制备及其在调Q掺铒光纤激光器中的应用
- Preparation of ultrathin ReS₂ nanosheets and their application to Q-switched Er-doped fiber lasers
- 信息与电子工程前沿（英文） 2021年22卷第3期页码：296-302
- Affiliations：
  
  School of Materials and Energy, Guangdong University of Technology, Guangzhou 510006, China
  State Key Laboratory of Luminescent Materials and Device, South China University of Technology, Guangzhou 510641, China
  Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques, South China University of Technology, Guangzhou 510641, China
  Guangdong Engineering Technology Research and Development Center of Special Optical Fiber Materials and Devices, South China University of Technology, Guangzhou 510641, China
- Author bio：
  
  Lili TAO, E-mail: taoll@gdut.edu.cn
  Bo ZHOU, E-mail: zhoubo@scut.edu.cn
- Funds：
  
  Project supported by the Pearl River Talent Program of Guangdong Province, China (No. 2017GC010278), the Science and Technology Program of Guangzhou, China (No. 202002030027), the National Natural Science Foundation of China (No. 61705044), and the Distinctive Innovation Project of Regular Colleges in Guangdong Province, China (No. 2018KTSCX052)
- DOI：10.1631/FITEE.2000339
  中图分类号： TN248;V254.2
- 收稿：2020-07-10，
  
  修回：2020-11-24，
  
  纸质出版：2021-03
- Accepted：
Scan QR Code
何俊杉, 曾国华, 刘绍贤, 等. 二硫化铼超薄纳米片的制备及其在调Q掺铒光纤激光器中的应用[J]. 信息与电子工程前沿（英文）, 2021,22(3):296-302.

Junshan HE, Guohua ZENG, Shaoxian LIU, et al. Preparation of ultrathin ReS₂ nanosheets and their application to Q-switched Er-doped fiber lasers[J]. Frontiers of Information Technology & Electronic Engineering, 2021, 22(3): 296-302.
何俊杉, 曾国华, 刘绍贤, 等. 二硫化铼超薄纳米片的制备及其在调Q掺铒光纤激光器中的应用[J]. 信息与电子工程前沿（英文）, 2021,22(3):296-302. DOI： 10.1631/FITEE.2000339.

Junshan HE, Guohua ZENG, Shaoxian LIU, et al. Preparation of ultrathin ReS₂ nanosheets and their application to Q-switched Er-doped fiber lasers[J]. Frontiers of Information Technology & Electronic Engineering, 2021, 22(3): 296-302. DOI： 10.1631/FITEE.2000339.

摘要

本文通过液相剥离法从自制二硫化铼粉末中制备二硫化铼超薄纳米片，并将其应用在调Q掺铒光纤激光器中。XRD、Raman和XPS表征结果证明具有层状结构二硫化铼的成功合成；通过SEM和AFM表征发现所制备的二硫化铼纳米片横向尺寸低于200 nm，厚度小于5 nm。将二硫化铼/PVA复合薄膜作为可饱和吸收体放入掺铒光纤激光器中可以获得调Q脉冲输出，脉冲宽度最窄为2.4 μs，输出功率为1.25 mW，揭示了二硫化铼在Q调制方面的潜在应用价值。

Abstract

We study the exfoliation of ultrathin ReS

nanosheets from the prepared ReS

powder and their application to Q-switched Er-doped fiber laser. XRD

Raman

and XPS spectra confirm the successful preparation of the layered ReS

. SEM images show that the obtained ReS

sheets have lateral size below 200 nm. The thickness of the ReS

nanosheets is smaller than 5 nm according to the AFM results. ReS

/PVA film is applied as a saturable absorber in an Er-doped Q-switched fiber laser

and a minimum pulse duration of 2.4 μs and an output power of 1.25 mW are obtained

indicating the potential application to Q-switched lasers.

关键词

Keywords

references

BH Chen , , , XY Zhang , , , K Wu , , , 等 . . Q-switched fiber laser based on transition metal dichalcogenides MoS 2 , MoSe 2 , WS 2 , and WSe 2 . . Opt Expr , , 2015 . . 23 ( ( 20 ): ): 26723 - - 26737 . . DOI: 10.1364/OE.23.026723 http://doi.org/10.1364/OE.23.026723 . .

YD Cui , , , FF Lu , , , XM Liu . . Nonlinear saturable and polarization-induced absorption of rhenium disulfide . . Sci Rep , , 2017 . . 7 40080 DOI: 10.1038/srep40080 http://doi.org/10.1038/srep40080 . .

J Du , , , QK Wang , , , GB Jiang , , , 等 . . Ytterbium-doped fiber laser passively mode locked by few-layer molybdenum disulfide (MoS 2 ) saturable absorber functioned with evanescent field interaction . . Sci Rep , , 2014 . . 4 6346 DOI: 10.1038/srep06346 http://doi.org/10.1038/srep06346 . .

L Du , , , GB Jiang , , , LL Miao , , , 等 . . Few-layer rhenium diselenide: an ambient-stable nonlinear optical modulator . . Opt Mater Expr , , 2018 . . 8 ( ( 4 ): ): 926 - - 935 . . DOI: 10.1364/OME.8.000926 http://doi.org/10.1364/OME.8.000926 . .

YQ Feng , , , W Zhou , , , YJ Wang , , , 等 . . Raman vibrational spectra of bulk to monolayer ReS 2 with lower symmetry . . Phys Rev B , , 2015 . . 92 ( ( 5 ): ): 054110 DOI: 10.1103/PhysRevB.92.054110 http://doi.org/10.1103/PhysRevB.92.054110 . .

J Guo , , , JL Zhao , , , DZ Hunag , , , 等 . . Two-dimensional tellurium-polymer membrane for ultrafast photonics . . Nanoscale , , 2019 . . 11 ( ( 13 ): ): 6235 - - 6242 . . DOI: 10.1039/C9NR00736A http://doi.org/10.1039/C9NR00736A . .

ZL Guo , , , AX Wei , , , Y Zhao , , , 等 . . Controllable growth of large-area atomically thin ReS 2 films and their thickness-dependent optoelectronic properties . . Appl Phys Lett , , 2019 . . 114 ( ( 15 ): ): 153102 DOI: 10.1063/1.5087456 http://doi.org/10.1063/1.5087456 . .

M Hafeez , , , L Gan , , , HQ Li , , , 等 . . Large-area bilayer ReS 2 film/multilayer ReS 2 flakes synthesized by chemical vapor deposition for high performance photodetectors . . Adv Funct Mater , , 2016 . . 26 ( ( 25 ): ): 4551 - - 4560 . . DOI: 10.1002/adfm.201601019 http://doi.org/10.1002/adfm.201601019 . .

JS He , , , LL Tao , , , H Zhang , , , 等 . . Emerging 2D materials beyond graphene for ultrashort pulse generation in fiber lasers . . Nanoscale , , 2019 . . 11 ( ( 6 ): ): 2577 - - 2593 . . DOI: 10.1039/C8NR09368G http://doi.org/10.1039/C8NR09368G . .

WC Huang , , , C Li , , , LF Gao , , , 等 . . Emerging black phosphorus analogue nanomaterials for high-performance device applications . . J Mater Chem C , , 2020 . . 8 ( ( 4 ): ): 1172 - - 1197 . . DOI: 10.1039/c9tc05558d http://doi.org/10.1039/c9tc05558d . .

X Huang , , , ZY Yin , , , SX Wu , , , 等 . . Graphene-based materials: synthesis, characterization, properties, and applications . . Small , , 2011 . . 7 ( ( 14 ): ): 1876 - - 1902 . . DOI: 10.1002/smll.201002009 http://doi.org/10.1002/smll.201002009 . .

D Jariwala , , , D Voiry , , , A Jindal , , , 等 . . Synthesis and characterization of ReS 2 and ReSe 2 layered chalcogenide single crystals . . Chem Mater , , 2016 . . 28 ( ( 10 ): ): 3352 - - 3359 . . DOI: 10.1021/acs.chemmater.6b00364 http://doi.org/10.1021/acs.chemmater.6b00364 . .

MX Lin , , , QQ Peng , , , W Hou , , , 等 . . 1.3 μm Q-switched solid-state laser based on few-layer ReS 2 saturable absorber . . Opt Laser Technol , , 2019 . . 109 90 - - 93 . . DOI: 10.1016/j.optlastec.2018.07.062 http://doi.org/10.1016/j.optlastec.2018.07.062 . .

EF Liu , , , MS Long , , , JW Zeng , , , 等 . . High responsivity phototransistors based on few-layer ReS 2 for weak signal detection . . Adv Funct Mater , , 2016 . . 26 ( ( 12 ): ): 1938 - - 1944 . . DOI: 10.1002/adfm.201504408 http://doi.org/10.1002/adfm.201504408 . .

F Liu , , , X Zhao , , , XQ Yan , , , 等 . . Ultrafast nonlinear absorption and carrier relaxation in ReS 2 and ReSe 2 films . . J Appl Phys , , 2019 . . 125 ( ( 17 ): ): 173105 DOI: 10.1063/1.5093757 http://doi.org/10.1063/1.5093757 . .

H Liu , , , AP Luo , , , FZ Wang , , , 等 . . Femtosecond pulse erbium-doped fiber laser by a few-layer MoS 2 saturable absorber . . Opt Lett , , 2014 . . 39 ( ( 15 ): ): 4591 - - 4594 . . DOI: 10.1364/OL.39.004591 http://doi.org/10.1364/OL.39.004591 . .

Y Liu , , , QW An , , , XQ Meng . . Controllable growth of vertical ReS 2 nanosheets and nanorods by vapor transport method . . J Mater Sci , , 2019 . . 54 ( ( 9 ): ): 6807 - - 6814 . . DOI: 10.1007/s10853-019-03395-x http://doi.org/10.1007/s10853-019-03395-x . .

ZQ Luo , , , YZ Huang , , , M Zhong , , , 等 . . 1-, 1.5-, and 2-μm fiber lasers Q-switched by a broadband few-layer MoS 2 saturable absorber . . J Lightw Technol , , 2014 . . 32 ( ( 24 ): ): 4679 - - 4686 . . DOI: 10.1109/jlt.2014.2362147 http://doi.org/10.1109/jlt.2014.2362147 . .

KF Mak , , , C Lee , , , J Hone , , , 等 . . Atomically thin MoS 2 : a new direct-gap semiconductor . . Phys Rev Lett , , 2010 . . 105 ( ( 13 ): ): 136805 DOI: 10.1103/PhysRevLett.105.136805 http://doi.org/10.1103/PhysRevLett.105.136805 . .

S Manzeli , , , D Ovchinnikov , , , D Pasquier , , , 等 . . 2D transition metal dichalcogenides . . Nat Rev Mater , , 2017 . . 2 ( ( 8 ): ): 17033 DOI: 10.1038/natrevmats.2017.33 http://doi.org/10.1038/natrevmats.2017.33 . .

D Mao , , , XQ Cui , , , XT Gan , , , 等 . . Passively Q-switched and mode-locked fiber laser based on an ReS 2 saturable absorber . . IEEE J Sel Top Quant Electron , , 2018 . . 24 ( ( 3 ): ): 1100406 DOI: 10.1109/JSTQE.2017.2713641 http://doi.org/10.1109/JSTQE.2017.2713641 . .

JK Qin , , , G Qiu , , , W He , , , 等 . . Epitaxial growth of 1D atomic chain based Se nanoplates on monolayer ReS 2 for high-performance photodetectors . . Adv Funct Mater , , 2018 . . 28 ( ( 48 ): ): 1806254 DOI: 10.1002/adfm.201806254 http://doi.org/10.1002/adfm.201806254 . .

XC Su , , , HK Nie , , , YR Wang , , , 等 . . Few-layered ReS 2 as saturable absorber for 2.8 μm solid state laser . . Opt Lett , , 2017 . . 42 ( ( 17 ): ): 3502 - - 3505 . . DOI: 10.1364/OL.42.003502 http://doi.org/10.1364/OL.42.003502 . .

LL Tao , , , XW Huang , , , JS He , , , 等 . . Vertically standing PtSe 2 film: a saturable absorber for a passively mode-locked Nd: LuVO 4 laser . . Photon Res , , 2018 . . 6 ( ( 7 ): ): 750 - - 755 . . DOI: 10.1364/PRJ.6.000750 http://doi.org/10.1364/PRJ.6.000750 . .

S Tongay , , , J Zhou , , , C Ataca , , , 等 . . Thermally driven crossover from indirect toward direct bandgap in 2D semiconductors: MoSe 2 versus MoS 2 . . Nano Lett , , 2012 . . 12 ( ( 11 ): ): 5576 - - 5580 . . DOI: 10.1021/nl302584w http://doi.org/10.1021/nl302584w . .

QH Wang , , , K Kalantar-Zadeh , , , A Kis , , , 等 . . Electronics and optoelectronics of two-dimensional transition metal dichalcogenides . . Nat Nanotechnol , , 2012 . . 7 ( ( 11 ): ): 699 - - 712 . . DOI: 10.1038/NNANO.2012.193 http://doi.org/10.1038/NNANO.2012.193 . .

SX Wang , , , HH Yu , , , HJ Zhang , , , 等 . . Broadband few-layer MoS 2 saturable absorbers . . Adv Mater , , 2014 . . 26 ( ( 21 ): ): 3538 - - 3544 . . DOI: 10.1002/adma.201306322 http://doi.org/10.1002/adma.201306322 . .

XY Wang , , , PK Cheng , , , CY Tang , , , 等 . . Laser Q-switching with PtS 2 microflakes saturable absorber . . Opt Express , , 2018 . . 26 ( ( 10 ): ): 13055 - - 13060 . . DOI: 10.1364/OE.26.013055 http://doi.org/10.1364/OE.26.013055 . .

CY Xing , , , ZJ Xie , , , ZM Liang , , , 等 . . 2D nonlayered selenium nanosheets: facile synthesis, photoluminescence, and ultrafast photonics . . Adv Opt Mater , , 2017 . . 5 ( ( 24 ): ): 1700884 DOI: 10.1002/adom.201700884 http://doi.org/10.1002/adom.201700884 . .

X Xu , , , M Jiang , , , D Li , , , 等 . . Passive Q-switching based on ReS 2 saturable absorber in Er-doped fiber laser at 1532 nm . . Opt Quant Electron , , 2018 . . 50 ( ( 1 ): ): 39 DOI: 10.1007/s11082-017-1281-3 http://doi.org/10.1007/s11082-017-1281-3 . .

LH Zeng , , , SH Lin , , , ZJ Li , , , 等 . . Fast, self-driven, air-stable, and broadband photodetector based on vertically aligned PtSe 2 /GaAs heterojunction . . Adv Funct Mater , , 2018 . . 28 ( ( 16 ): ): 1705970 DOI: 10.1002/adfm.201705970 http://doi.org/10.1002/adfm.201705970 . .

LH Zeng , , , D Wu , , , SH Lin , , , 等 . . Controlled synthesis of 2D palladium diselenide for sensitive photodetector applications . . Adv Funct Mater , , 2019 . . 29 ( ( 1 ): ): 1806878 DOI: 10.1002/adfm.201806878 http://doi.org/10.1002/adfm.201806878 . .

K Zhang , , , M Feng , , , YY Ren , , , 等 . . Q-switched and mode-locked Er-doped fiber laser using PtSe 2 as a saturable absorber . . Photon Res , , 2018 . . 6 ( ( 9 ): ): 893 - - 899 . . DOI: 10.1364/PRJ.6.000893 http://doi.org/10.1364/PRJ.6.000893 . .

M Zhang , , , GH Hu , , , GQ Hu , , , 等 . . Yb- and Er-doped fiber laser Q-switched with an optically uniform, broadband WS 2 saturable absorber . . Sci Rep , , 2015 . . 5 17482 DOI: 10.1038/srep17482 http://doi.org/10.1038/srep17482 . .

Y Zhang , , , TR Chang , , , B Zhou , , , 等 . . Direct observation of the transition from indirect to direct bandgap in atomically thin epitaxial MoSe 2 . . Nat Nanotechnol , , 2014 . . 9 ( ( 2 ): ): 111 - - 115 . . DOI: 10.1038/NNANO.2013.277 http://doi.org/10.1038/NNANO.2013.277 . .

浏览量

Downloads

CSCD

文章被引用时，请邮件提醒。

Submit

工具集

关联资源

Passive mode-locked Er-doped fiber laser pulse generation based on titanium disulfide saturable absorber